A single stage process for the preparation of cycotetramethylene tetranitrmine

Authors

  • H. K. Acharya Explosive Research & Development Laboratory, Kirkee
  • R. T. Limaye Explosive Research & Development Laboratory, Kirkee

DOI:

https://doi.org/10.14429/dsj.14.7204

Keywords:

Cyclotetramethylene, Tetranitramine

Abstract

A single stage process for the preparation of cyclotetrmethlene tetranitramine (HMX)has been developed. The ingredients (i) Hexamine in glacial acetic acid, (ii) Ammonium nitrate in nitric acid and (iii)acetic anhydride were simultaneously added to glacial acetic acid medium maintained at 45-48 with stirring. The crude yield of the product per 100 gm. of hexamine used is 120 gm having the melting point 265-266C. Purified from acetone the substance melts at 272-275 and passes standard vacuum stability and impact sensitivity tests.

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Published

2014-05-15

How to Cite

Acharya, H. K., & Limaye, R. T. (2014). A single stage process for the preparation of cycotetramethylene tetranitrmine. Defence Science Journal, 14(4), 325–328. https://doi.org/10.14429/dsj.14.7204

Issue

Vol. 14 No. 4

Section

Research Papers

License

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